Design and characterisation of metallic glassy alloys of high neutron shielding capability

This paper reports the design, making and characterisation of a series of Fe-based bulk metallic glass alloys with the aim of achieving the combined properties of high neutron absorption capability and sufficient glass forming ability. Synchrotron X-ray diffraction and pair distribution function methods were used to characterise the crystalline or amorphous states of the samples. Neutron transmission and macroscopic attenuation coefficients of the designed alloys were measured using energy resolved neutron imaging method and the very recently developed microchannel plate detector. The study found that the newly designed alloy (Fe48Cr15Mo14C15B6Gd2 with a glass forming ability of Ø5.8 mm) has the highest neutron absorption capability among all Fe-based bulk metallic glasses so far reported. It is a promising material for neutron shielding applications

A high resolution, high frame rate detector based on a microchannel plate read out with the Medipix2 counting CMOS pixel chip.

The future of ground-based optical astronomy lies with advancements in adaptive optics (AO) to overcome the limitations that the atmosphere places on high resolution imaging. A key technology for AO systems on future very large telescopes are the wavefront sensors (WFS) which detect the optical phase error and send corrections to deformable mirrors. Telescopes with >30 m diameters will require WFS detectors that have large pixel formats (512x512), low noise (<3 e-/pixel) and very high frame rates (~1 kHz). These requirements have led to the idea of a bare CMOS active pixel device (the Medipix2 chip) functioning in counting mode as an anode with noiseless readout for a microchannel plate (MCP) detector and at 1 kHz continuous frame rate. First measurement results obtained with this novel detector are presented both for UV photons and beta particles

CalFUSE v3: A Data-Reduction Pipeline for the Far Ultraviolet Spectroscopic Explorer

Since its launch in 1999, the Far Ultraviolet Spectroscopic Explorer (FUSE) has made over 4600 observations of some 2500 individual targets. The data are reduced by the Principal Investigator team at the Johns Hopkins University and archived at the Multimission Archive at Space Telescope (MAST). The data-reduction software package, called CalFUSE, has evolved considerably over the lifetime of the mission. The entire FUSE data set has recently been reprocessed with CalFUSE v3.2, the latest version of this software. This paper describes CalFUSE v3.2, the instrument calibrations upon which it is based, and the format of the resulting calibrated data files.Comment: To appear in PASP; 29 pages, 13 figures, uses aastex, emulateap

A noiseless kilohertz frame rate imaging detector based on microchannel plates read out with the Medipix2 CMOS pixel chip

A new hybrid optical imaging detector is described that is being developed for the next generation adaptive optics (AO) wavefront sensors (WFS) for ground-based telescopes. The detector consists of a photocathode and proximity focused microchannel plates (MCPs) read out by the Medipix2 CMOS pixel ASIC. Each pixel of the Medipix2 device measures 55x55 um2 and comprises pre-amplifier, a window discriminator and a 14-bit counter. The 256x256 Medipix2 array can be read out noiselessly in 287 us. The readout can be electronically shuttered down to a temporal window of a few us. The Medipix2 is buttable on 3 sides to produce 512x(n*256) pixel devices. Measurements with ultraviolet light yield a spatial resolution of the detector at the Nyquist limit. Sub-pixel resolution can be achieved using centroiding algorithms. For the AO application, very high continuous frame rates of the order of 1 kHz are required for a matrix of 512x512 pixels. The design concepts of a parallel readout board are presented that will allow this fast data throughput. The development status of the optical WFS tube is also explained

Antiferromagnetic real-space configuration probed by x-ray orbital angular momentum phase dichroism

X-ray beams with orbital angular momentum (OAM) are an up-and-coming tool for x-ray characterization techniques. Beams with OAM have an azimuthally varying phase that leads to a gradient of the light field. New material properties can be probed by utilizing the unique phase structure of an OAM beam. Here, we demonstrate a novel type of phase dichroism in resonant diffraction from an artificial antiferromagnet with a topological defect. The scattered OAM beam has circular dichroism whose sign is coupled to the phase of the beam, which reveals the real-space configuration of the antiferromagnetic ground state. Thermal cycling of the artificial antiferromagnet can change the ground state, as indicated by the changing phase dichroism. These results exemplify the potential of OAM beams to probe matter in a way that is inaccessible using typical x-ray techniques

<i>In situ</i> diagnostics of the crystal-growth process through neutron imaging:application to scintillators

Neutrons are known to be unique probes in situations where other types of radiation fail to penetrate samples and their surrounding structures. In this paper it is demonstrated how thermal and cold neutron radiography can provide time-resolved imaging of materials while they are being processed (e.g. while growing single crystals). The processing equipment, in this case furnaces, and the scintillator materials are opaque to conventional X-ray interrogation techniques. The distribution of the europium activator within a BaBrCl:Eu scintillator (0.1 and 0.5% nominal doping concentrations per mole) is studied in situ during the melting and solidification processes with a temporal resolution of 5-7 s. The strong tendency of the Eu dopant to segregate during the solidification process is observed in repeated cycles, with Eu forming clusters on multiple length scales (only for clusters larger than ∼50 µm, as limited by the resolution of the present experiments). It is also demonstrated that the dopant concentration can be quantified even for very low concentration levels (∼0.1%) in 10 mm thick samples. The interface between the solid and liquid phases can also be imaged, provided there is a sufficient change in concentration of one of the elements with a sufficient neutron attenuation cross section. Tomographic imaging of the BaBrCl:0.1%Eu sample reveals a strong correlation between crystal fractures and Eu-deficient clusters. The results of these experiments demonstrate the unique capabilities of neutron imaging for in situ diagnostics and the optimization of crystal-growth procedures

Synchrotron Microtomography and Neutron Radiography Characterization of the Microstruture and Water Absorption of Concrete from Pompeii

There is renewed interest in using advanced techniques to characterize ancient Roman concrete. In the present work, samples were drilled from the "Hospitium" in Pompeii and were analyzed by synchrotron microtomography (uCT) and neutron radiography to study how the microstructure, including the presence of induced cracks, affects their water adsorption. The water distribution and absorptivity were quantified by neutron radiography. The 3D crack propagation, pore size distribution and orientation, tortuosity, and connectivity were analyzed from uCT results using advanced imaging methods. The concrete characterization also included classical methods (e.g., differential thermal-thermogravimetric, X-ray diffractometry, and scanning electron microscopy). Ductile fracture patterns were observed once cracks were introduced. When compared to Portland cement mortar/concrete, Pompeii samples had relatively high porosity, low connectivity, and similar coefficient of capillary penetration. In addition, the permeability was predicted from models based on percolation theory and the pore structure data to evaluate the fluid transport properties

Single photon imaging at ultra-high resolution

Abstract We present a detection system capable of imaging both single photon/positive ion and multiple coincidence photons/positive ions with extremely high spatial resolution. In this detector the photoelectrons excited by the incoming photons are multiplied by microchannel plate(s) (MCP). The process of multiplication is spatially constrained within an MCP pore, which can be as small as 4 μm for commercially available MCPs. An electron cloud originated by a single photoelectron is then encoded by a pixellated custom analog ASIC consisting of 105 K charge sensitive pixels of 50 μm in size arranged on a hexagonal grid. Each pixel registers the charge with an accuracy o